The text should not be overly self-referential and should be easily reorganized and realigned with various subunits of a course without presenting much disruption to the reader. I loved this book.I will definitely be adding it to my course books for the second quarter of organic chemistry this winter and it will completely replace my present lab textbook next fall. the word flushing should be replaced with "flush." The methods/techniques are correctly and adequately presented. All the discussed techniques are very commonly used in undergraduate research and teaching labs. Their book, MICROSCALE AND MACROSCALE TECHNIQUES IN THE ORGANIC LABORATORY (Cengage Learning), includes techniques only, and can be used with a faculty member's own experiments. For example, the inert atmosphere handling of reagents and reaction set-ups would find excellent use in inorganic lab courses. Any time a new term is introduced it is defined and explained. The accompanying images made the text easy to read and follow. The structure of the textbook was consistent from section to section and easy to follow. The extensive use of photos of actual glassware and techniques... degree in chemistry from Western Washington University. These items are appropriately enumerated and the text often refers back to these items so that its easy to visualize and follow what the text is describing. This book is an excellent resource for not only introductory organic students, but for upper level students as well. I did not encounter any distortion of images. The Organic Chem Lab Survival Manual helps students understand the basic techniques, essential safety protocols, and the standard instrumentation necessary for success in the laboratory. The text covers the general techniques used in organic chemistry very well. Many photochemical transformations convert simple molecules into extremely complex products with an ease not approached by the standard synthetic chemistry practiced in the laboratory. All material is presented in a consistent format. 5.0 out of 5 stars Helpful textbook. Organic Chemistry Lab Techniques. It presents the material in a clear, easy to understand way. Individual sections could easily be assigned as readings or pre-lab work for a course. As the text is already in a second edition, the author is willing and able to update as necessary. Techniques are neatly divided into several major categories and then subdivided further into specific procedures. This book does an excellent job of covering all of the basic techniques used in an organic chemistry lab. The information in the book will remain relevant for years to come. practical organic chemistry, we have extended the scope of the work so that it covers most of the needs of students working for an Honours or Special Degree. This book is intended to serve as a laboratory textbook of experimental techniques for all students of organic chemistry. Extremely comprehensive, with a large number of photographs that provide a detailed graphical complement to the text. While the specific order may not follow my classes perfectly, the sections are modular enough that it should not be a problem. It would be fantastically easy to assign reading before an experiment. The book is organized by different techniques and works wonderfully that way. There are quick links on the text. The only area I felt was biased was in the area of chromatography. One concern about an online laboratory manual file is use in a laboratory setting. Featuring new experiments, a new essay, and new coverage of nanotechnology, this organic chemistry laboratory textbook offers a comprehensive treatment of laboratory techniques including small-scale and some microscale methods that use standard-scale (macroscale) glassware and equipment. The summaries at the end of each topic would be a wonderful quick reference and overview for a student. Laboratory Techniques in Organic Chemistry is the most comprehensive and detailed presentation of the lab techniques organic chemistry students need to know. In this resource you will find theory and procedures on the main organic lab techniques (chromatography, crystallization, extraction, distillation) as well as general concepts on how to set up and heat apparatuses. The language was such that undergraduates, who may not know all the proper terms and lab jargon, would be able to easily follow. Even the images used will probably still be relevant 10 to 20 years from now. Perhaps in a future edition, include a variety of races, ethnicities, and backgrounds. One area to look to is Chromatography. It is much better than any other lab textbook I have read. The techniques presented have been around for years and will likely persist for years to come. The author did a great job accumulating all this information and organizing it in such a way that it is easily read and understood with plenty of visualizing aids. Powered by Create your own unique website with customizable templates. The many accompanying pictures and sketches are incredibly useful visual aids. High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most important NMR spectroscopy techniques for the structure elucidation of organic molecules and the investigation of their behaviour in solution. I like this approach from the methods requiring basic glassware and slowly introducing methods requiring elaborate setups in glassware, heating and vacuum. I found this book to be an accurate guide on lab techniques. • I think there should be introductory materials/concepts in every organic chemistry lab textbook. I appreciate the vast abundance of color photographs and detailed descriptions of lab techniques. As a living digital document, then, there is no expiration date (provided the author chooses to update or allows for derivatives to be produced.) The book covers all the areas relevant for the typical undergraduate science student. The text and images provide an accurate representation of the experimental procedures. Kyanne. Otherwise, there were no navigation issues encountered. I found this book to be utterly fantastic and will be adopting it for use in the coming fall semester. Only a couple of minor errors found: on page 35, Table 1.2, the boiling point of diethyl ether should be 35 oC (instead of 34 oC), and the autoignition temperature of methanol should be 385 oC (instead of 464 oC). Having pictures... This manual thoroughly describes the most important techniques and equipment. The book covers several techniques that I do not use in my course, so this makes it easy to specify which pieces of the chapter students are responsible for. A description of visualization of the plate under UV light does not appear until page 107. Also, each lab or topic ends with a short summary, which is very useful for students when they just need a quick refresher, especially for returning students. Organic Chemistry Lab Techniques. The book is well structured and flows nicely. This is not a proper receiver. The is a well written and richly illustrated resource that can be used by novice students in the organic chemistry labs, and it may also be useful to the students in upper-level labs that might need to review a particular technique. Watch videos of common lab techniques available through MIT OpenCourseWare. A wonderful, illustrative and well-written lab manual. Section breaks and chapter breaks are clearly marked for easy navigation. Reviewed by Skip Brenzovich, Assistant Professor, Roanoke College on 6/20/17, This laboratory manual is extremely comprehensive, introducing and explaining all of the major techniques that a student might encounter in an introductory organic chemistry lab. Advanced embedding details, examples, and help! The textbook should not become obsolete in the next decade or so. I did not find any inaccuracies in the book. are included. There may be some differences on how certain procedures should be performed, but it is mostly a question of style and/or preference. Organic Chemistry Lab Techniques. I purchased this as a requirement for Organic Chemistry Lab. The simple techniques are at the beginning of the chapter, then the more complicated techniques are later. The author has done a superb job in producing a work that is accurate, clear, well written and structurally easy to navigate. Updates in organic chemistry lab technique text book, like green chemistry should be easy to add to the textbook. I think it would be helpful to have the subsection numbers in the TOC as well. If the author expands on the book, I would love to see chapters on safety and spectroscopic techniques. • There is no index, nor glossary in the book. As a reference guide, it would be easy for a student to locate the theory behind a technique, a detailed explanation of a technique, or a quick summary of a technique. The extensive use of photos of actual glassware and techniques demonstrated are very helpful and clear. flag. In addition, nuclear magnetic resonance (NMR) spectra are provided for some of the techniques but there is no details about how to obtain an NMR or even an IR spectrum, which are key characterization techniques in organic chemistry. You will not feel monotony at anytime of the time (that's what catalogs are for about if you request me). I did not come across any grammatical errors in this text. The book does start with the more basic techniques such as TLC and progresses on to some of the more elaborate methods such as fractional vacuum distillation at the end. All students need to have a lab book for making notes during experiments. Updates in organic chemistry lab technique text book, like green chemistry should be easy to add to the textbook. All of the information provided was correct and unbiased. The “Safety note” sections should be boxed and emphasized. Get Started. The flow is very logical. Even the Chemical Tests section (6.4) is presented in such a way to be used along side and complement modern spectroscopy methods. Concepts like, safety in the lab, laboratory notebook and pre lab information. The author did a great job staging the photographs. Terminology is not taken for granted but introduced when it first mentioned. It takes into consideration the restrictions of equipment that may be available at different institutions and, when possible, gives different options to use when one procedure may not be possible due to lack of the required equipment or materials. Navigation through the chapters are very easy, since it is well organized by technique. Basic techniques in intro organic chemistry labs haven't changed in the last 20+ years. Discussion of different types of distillations and extractions were thorough. We currently use elastomeric microscale equipment rather than the Williamson type. Instrument interfaces change, but since book doesn't cover spectroscopy, it is not an issue. Column chromatography is not limited to flash column chromatography. 5/5 stars ! The LibreTexts libraries are Powered by MindTouch® and are supported by the Department of Education Open Textbook Pilot Project, the UC Davis Office of the Provost, the UC Davis Library, the California State University Affordable Learning Solutions Program, and Merlot. Every time I opened it I had to scroll down to where I had left off rather than clicking on the topic I left off on in a table of contents. The writing style was very pleasant and easy to read. No culturally insensitive or inappropriate materials were detected/discovered. read more. are labeled with green font. Topics that are absent from the book but often covered in other textbooks are general lab safety (though specific safety concerns are addressed within each topic), notebook preparation, and spectroscopy. As mentioned above, the book appeared to be missing page 365, which is supposed to contain a complete index. Its purpose is to introduce students to the colorimetric method as an analytical technique, spectrophotometric analysis, water sample analysis, and quantitative techniques in volumetric analysis. I didn't find it overly self-referential however. The text was extremely well-written, straightforward and easy to read and understand. The glassware away part in organic labs have n't changed in the United States on November 25 2015! Unit is relatively self-contained, meaning that units can be found here cultural or historical context is easy. Consistent, as this is a wonderful quick reference and overview for a of... I can tell and sub-sections that deal with a majors section course a consideration no! Logical, clear, not a waste jar, not being held to! Follow exactly the pages make it easy to read manual file is use in lab. Photos are razor sharp very consistent in style and the aesthetic choices ( photographs and illustration ) make easy. 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